NMR - From Spectra to Structures

Nuclear magnetic resonance spectroscopy is one of the most powerful analytical methods. This practice-oriented textbook aims at teaching how NMR experiments should be used to make structural asssignments. The book is intended as a practical guide for students and laboratory personnel, so that the emphasis is on practical rather than on theoretical aspects, which are treated only to the extent necessary to understand the experiments and to interpret the results. The second edition has been expanded to include several other heteronuclei (15N, 19F, 29Si, 77Se, 113Cd, 117Sn/119Sn, 195Pt, 207Pb) and a new chapter on solid state NMR. The problems section has been enlarged and now includes 50 problems. These are of different degrees of complexity and in all cases include two-dimensional (2D) methods as well as standard proton and carbon 1D spectra.

Auteur

Introduction

Part I - NMR Experiments

1. 1D Experiments

2. 2D Experiments

3. Quadrupolar Nucleus Experiments

4. HPLC-NMR Coupling

Appendix: Reference List

Part II - Worked Example and Problems

Introduction

Worked Example

Problems

Index

Texte du rabat

This practice-oriented textbook shows how to utilize the huge variety of NMR experiments available today in addition to standard experiments. Intended as a practical guide for students and laboratory personnel, it treats theoretical aspects only to the extent necessary to understand the experiments and to interpret the results.

The book is significantly revised and expanded for the 2nd edition, and now includes the nuclei 1H/2H, 13C, 31P, 17O, 15N, 19F, 29Si, 77Se, 113Cd, 117Sn/119Sn, 195Pt, 207Pb and a new chapter on solid state NMR. An expanded set of 50 graded problems offers invaluable help for students, practitioners and laboratory personnel alike.

Contenu

Introduction.- Part I - NMR Experiments.- 1D Experiments.- 2D Experiments.- Quadrupolar Nucleus.- Experiments.- HPLC-NMR Coupling.- Appendix: Reference List.- Part II - Worked Example and Problems.- Introduction.- Worked Example.- Problems.