Green Chemical Analysis and Sample Preparations

This volume focuses on the most recent trends for greening analytical activities beginning with an introduction to green analytical chemistry followed by a discussion of green analytical chemistry metrics and life-cycle assessment approach to analytical method development. The chapters discuss two main topics; first is the most recent techniques for greening sample pretreatment steps, and second is modern trends for tailoring analytical techniques and instrumentation to implement the green analytical chemistry concept. The role of different kinds of green solvents, such as ionic liquids, supercritical fluids, deep eutectic solvents, bio-based solvents, and surfactants, as well as nanomaterials and green sorption materials in greening sample extraction steps is also a focus of this book. Furthermore, different approaches for greening chromatography as a key analytical technique are discussed. The applications of nanomaterials in analytical procedures are deeply reviewed, and miniaturization of spectrometers is also discussed as a recently evolved approach for efficient green on-site analysis. This book will appeal to a wide readership of academic and industrial researchers in different fields. It can be used in the classroom for undergraduate and postgraduate students focusing on the development of new analytical procedures for organic and inorganic compounds determination in different kinds of samples characterized by complex matrices composition. The book will also be useful for researchers that are interested in both chemical analysis and environment protection.

Auteur

Dr. Mahmoud El-Maghrabey has been an Associate Professor in the Department of Pharmaceutical Analytical Chemistry, Faculty of Pharmacy - Mansoura University, Egypt since 2022 & an Assistant Professor in the Graduate School of Biomedical Sciences - Nagasaki University, Japan, since 2020. He his Ph.D. degree from the Graduate School of Biomedical Sciences, Nagasaki University, Japan. Then, He was awarded many prestigious post-doctoral fellowships, including Takeda Science Foundation Fellowship in 2017 and JSPS Fellowship in 2018. He was a visiting researcher at the Graduate School of Biomedical Sciences, Nagasaki University, in the period of 2017-2020. His research focuses on developing new green detecting probes for bioactive substances, including pharmaceuticals and their potential impurities, metals, and pollutants. Besides, He developed many probes for mass spectrometric, fluorescence, and chemiluminescence analysis of clinically important compounds. He has published more than 30 research articles in esteemed Peer-Reviewed journals and eight book chapters published by highly esteemed publishers, including Springer. He established many collaborative research with professors and researchers from many countries around the world, including Japan, Hungary, Spain, Australia, France, Egypt, Saudi Arabia, Taiwan, Iraq, and India.

Dr. V. Sivasankar has been an Assistant Professor in the Post Graduate and Research Department of Chemistry at Pachaiyappa's College (affiliated to the University of Madras), Chennai, India, since 2014. He received his doctorate in Chemistry in 2009 from Bharathidasan University at Tiruchirappalli, India. He was a JSPS Post-Doctoral Fellow in 2016 from Nagasaki University in Nagasaki, Japan. His research areas include materials synthesis and wastewater treatment. To his credit, he has more than 70 research articles in Peer-Reviewed journals and seven book chapters in renowned publishers. He edited books on Surface Modified Carbons as Scavengers of Fluoride from Water (2016), Microbial Fuel Cell Technology for Bio-electricity (2018), and Organic Pollutants - Toxicity and Solutions (2021) with Springer. He collaborates and performs research with professors in universities and research laboratories in Algeria, France, Japan, Iran, and South Africa.

Dr. Rania El-Shaheny has been a Professor at the Pharmaceutical Analytical Chemistry Department, Faculty of Pharmacy, Mansoura University, Since 2022. She received her Ph.D. degree from the Faculty of Pharmacy, Mansoura University, Egypt. Then, She was awarded many prestigious post-doctoral fellowships and missions, including a scientific mission from the Egyptian Cultural Affairs and Mission Sectors (Egyptian Ministry of Higher Education) in 2013 and a Fellowship from Takeda Science Foundation in 2018. She was a visiting researcher at the Graduate School of Biomedical Sciences, Nagasaki University, in the periods of 2013-2014 and 2018-2021. Her research focuses on the development of new environmentally benign luminescence-based probes for clinically significant compounds in addition to developing probes for pharmaceuticals and environmental pollutants. Besides, her research interests included the usage of nanomaterials as nano extraction beds and nanoprobes for pharmaceuticals. Furthermore, her research included developing novel analytical techniques for investigating the safety, pharmacokinetics, and in vivo transformations of drugs. She has published more than 40 research articles in esteemed Peer-Reviewed journals and eight book chapters published by highly esteemed publishers, including Springer. She established many collaborative research with professors and researchers from many countries around the world, including Japan, Hungary, Egypt, Saudi Arabia, Iraq, and India.

Contenu

1-Introduction to green analytical chemistry.- 2-Green analytical chemistry metrics and Life-cycle assessment approach to analytical method development.- 3-Greening analytical Chemistry by chemometrics.- 4-Integration and automation of analytical processes and operations.- 5-In situ measurements and on line measurements for greener analysis.- 6-Liquid-phase microextraction as a greener extraction tool.- 7-Ionic liquids as greener solvents for sample pre-treatment of environmental, pharmaceutical, and biological samples.- 8-Ionic liquids for greener extraction of precious metals.- 9-Deep eutectic solvents, bio-based solvents, and surfactants for green sample pretreatment and determination.- 10-Applications of nanomaterials for greener sample extraction.- 11-Green sorption materials used in analytical procedures.- 12-Recent approaches for greening sample derivatization.- 13-Green chromatography techniques.- 14-Applications of nanomaterials for greener determination of environmental contaminants.- 15-Applications of nanomaterials for greener determination of pharmaceutical and biological molecules.- 16-Applications of nanomaterials for greener food analysis.