NMR - From Spectra to Structures

This practice-oriented textbook teaches how to use magnetic resonance spectroscopy - one of the most powerful analytical methods available showing how to utilize the huge variety of NMR experiments available today in addition to the standard experiments. The book is intended as a practical guide for students and laboratory personnel. Therefore, the emphasis is on practical rather than on theoretical aspects, which are treated only to the extent necessary to understand the experiments and to interpret the results.

The book has been significantly revised and expanded for the 2nd edition, and now includes the nuclei 1 H/ 2 H, 13 C, 31 P, 17 O, 15 N, 19 F, 29 Si, 77 Se, 113 Cd, 117 Sn/ 119 Sn, 195 Pt, 207 Pb and a new chapter on solid state NMR. An expanded set of 50 graded problems in the problems section supports understanding of how problems in structure elucidation are solved by using NMR offers invaluable help for students, practitioners and laboratory personnel alike.

The practical guide to today's NMR experiments aims at teaching how to use the huge variety of NMR experiments available today The emphasis is on practical rather than on theoretical aspects Now includes the nuclei 1H/2H, 13C, 31P, 17O, 15N, 19F, 29Si, 77Se, 113Cd, 117Sn/119Sn, 195Pt, 207Pb and a new chapter on solid state NMR The collection of 50 problems of different complexity is an invaluable help for students, practitioners and laboratory personnel Includes supplementary material: sn.pub/extras

Auteur

Introduction

Part I - NMR Experiments

1. 1D Experiments

2. 2D Experiments

3. Quadrupolar Nucleus Experiments

4. HPLC-NMR Coupling

Appendix: Reference List

Part II - Worked Example and Problems

Introduction

Worked Example

Problems

Index

Texte du rabat

Nuclear magnetic resonance spectroscopy is one of the most powerful analytical methods. This practice-oriented textbook aims at teaching how NMR experiments should be used to make structural asssignments. The book is intended as a practical guide for students and laboratory personnel, so that the emphasis is on practical rather than on theoretical aspects, which are treated only to the extent necessary to understand the experiments and to interpret the results.
The second edition has been expanded to include several other heteronuclei (15N, 19F, 29Si, 77Se, 113Cd, 117Sn/119Sn, 195Pt, 207Pb) and a new chapter on solid state NMR. The problems section has been enlarged and now includes 50 problems. These are of different degrees of complexity and in all cases include two-dimensional (2D) methods as well as standard proton and carbon 1D spectra.

Contenu
NMR Experiments.- 1D Experiments.- 2D Experiments.- Quadrupolar Nucleus Experiments.- HPLC-NMR Coupling.- Other Spin-1/2 Nuclei.- Solid State NMR.- Worked Example and Problems.- Section 1.- Worked Example.- Problems.- Section 2.